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Download Analysis, Networks, Peptides by K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. PDF

By K. Bode, I. Kuriyama, J.E. Mark, F. Maser, M. Mutter, Y. Nakose, A. Odajima, V.N.R. Pillai, J.P. Queslel, H.W. Siesler

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The maximum extent of disruption according to Fig. 15 is reached at the lowest stress level beyond the yield point at about 150 % strain (Fig. 13 b). Further elongation finally leads to a reincrease of both stress and proportion of orthorhombic crystal phase. The aforementioned structural changes occurring during uniaxial elongation at 300 K are additionally superimposed by a crystal phase transformation. 1- a-b 4o 760 a wavenumbers a b z6o wavenumbers Fig. 16a and b. W. Siesler T 'd I 680 700 1 :5 o E t 720 740 wovenumbers 10o_ I Fig.

To correlate the macroscopic properties and the structural changes occurring during deformation the orientation functions evaluated from Eqs. (20a--c) have been plotted in dependence of strain in Fig. 14. Onogi and Asada ~) have discussed in detail the expected changes of infrared dichroism and orientation functions due to the different molecular processes of lamellar orientation and chain unfolding. W. 5. 1. a 7507O0 7507OO wavenumbers 25t 201 ~ 300K N b 100 200 300 strain (%) 460 Fig. 131. 4- Fig.

From the orientation and dichroic functions of the 1126 cm -1 and 1662 cm -1 bands, respectively, an average inclination angle of approximately 35 ° was calculated for the polymer chains of the crystal phase and the direction of stretch whereas a value of about 44° was determined for the chain alignment of the amorphous polymer in the 530 % drawn sample. W. Siesler 10 to ,,........... " e (s) 2 100 200 300 400 50-O-strain (%) TOO Fig. 41. 0 • •eeeu. . . . 6 ~ ~, N AA• • • AA~ • • ]lA~Aal • ...

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